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KMID : 0385520170300010020
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Analytical Science & Technology
2017 Volume.30 No. 1 p.20 ~ p.25
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Simultaneous determination of bisphenol A, chlorophenols and alkylphenols by solid-phase extraction and HPLC
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Lee Tae-Joon
Park Keun-Young
Pyo Dong-Jin
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Abstract
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An analytical method for determining potential endocrine disruptors (bisphenol A, 2-chlorophenol, 2,4-dichlorophenol, 2,4,6-trichlorophenol, pentachlorophenol, p-t-butylphenol, p-pentylphenol, p-hexylphenol, pt-octylphenol, p-heptylphenol, nonylphenol) by solid-phase extraction (SPE) and High Perfomance Liquid Chromatography(HPLC) equipped with fluorescence and variable wavelength detector has been developed. The SPE process for sample concentration was performed on a commercially available Oasis HLB cartridge packed with polymeric sorbents. The effect of elution solvent and elution volume on the recoveries of the analytes were investigated with HPLC. Average recovery of >85% was achieved with 60mg sorbents using 5mL of methanol as elution solvent. Phenolic compounds in canned drinks, beverages and water samples were surveyed by this proposed method.
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KEYWORD
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bisphenol A, alkylphenols, chlorophenols, high performance liquid chromathgraphy (HPLC), solid phase extraction (SPE)
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